Publications

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Journal Articles


2024

Gaseous inhibitors: A comprehensive overview on mitigating hydrogen embrittlement in pipeline steels

Published in International Journal of Hydrogen Energy, 2024

This work reviews hydrogen embrittlement risks in pipeline steels during hydrogen transport and explores mitigation using trace inhibitor gases like oxygen and carbon monoxide. It examines surface interactions, showing inhibitors slow hydrogen adsorption but cannot stop equilibrium absorption, requiring continuous supply. The study highlights how factors such as test type, pressure, and inhibitor concentration affect mitigation effectiveness.

Recommended citation: Jubica, L. Claeys, A. Laureys, W. De Waele, J. Schweicher, T. Depover, K. Verbeken, Gaseous inhibitors: A comprehensive overview on mitigating hydrogen embrittlement in pipeline steels, International Journal of Hydrogen Energy 136 (2025) 630-642. doi:10.1016/j.ijhydene.2024.08.018
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Conference Papers


2025

Role of gaseous charging parameters on hydrogen uptake in pipeline steels

Published in 5th International Conference on Metals and Hydrogen 2025, Ghent, 2025

This study investigates the effect of gaseous charging parameters on the hydrogen uptake of pipeline steels, as presented at the 5th International Conference on Metals and Hydrogen.

Recommended citation: J. Jubica, L. Claeys, J. Schweicher, W. De Waele, K. Verbeken, and T. Depover, "Role of gaseous charging parameters on hydrogen uptake in pipeline steels," in 5th International Conference on Metals and Hydrogen 2025, Book of Abstracts, Ghent, 2025.
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Linking microstructure to fracture morphology under hydrogen charging in L485MB pipeline steels

Published in The Energy Pipeline Innovation Conference (EPIC 2025), Cambridge, United Kingdom, 2025

Hydrogen affects the mechanical properties of pipeline steels. The underlying microstructure often governs the severity of hydrogen-assisted degradation. This work uses ex-situ quasi-static tensile tests to study the hydrogen performance of two cold-bent L485MB pipeline steels with different banding morphologies.

Recommended citation: J. Jubica et al., "Linking microstructure to fracture morphology under hydrogen charging in L485MB pipeline steels," in Proceedings of the Energy Pipeline Innovation Conference 2025, Cambridge, United Kingdom, 2025.
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A comprehensive overview of hydrogen transport in existing pipelines and mitigation of hydrogen embrittlement by gaseous inhibitors

Published in EUROCORR 2025, Abstracts, Stavanger, Norway, 2025

The transition of existing natural gas infrastructures to transportation and storage of sustainable hydrogen gas is crucial for the global decarbonization of the energy sector. However, hydrogen absorption in pipeline steels can degrade their mechanical properties, necessitating prior confirmation of the fitness-for-service of existing pipelines for pressurized hydrogen transport. This work presents a literature overview on the relevant aspects of hydrogen embrittlement (HE) in pipeline steels and its mitigation through addition of inhibitors. Hydrogen-assisted fatigue crack growth, which occurs under cyclic loading even at low hydrogen partial pressures, is considered to be a significant failure mode in pipeline steels transporting hydrogen gas, leading to potential lifetime reduction. Mechanical, environmental and material variables can all influence the severity of HE. Gaseous additives, such as oxygen or carbon monoxide, have shown potential in mitigating HE by slowing hydrogen adsorption kinetics. However, sustained mitigation requires continuous supply of these inhibitors.

Recommended citation: A. Laureys, Jubica, M. Cauwels, L. Claeys, W. De Waele, T. Depover, & K. Verbeken, “A comprehensive overview of hydrogen transport in existing pipelines and mitigation of hydrogen embrittlement by gaseous inhibitors,” in EUROCORR 2025, Abstracts, Stavanger, Norway, 2025.
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2024

Hydrogen embrittlement in L485 pipeline materials : comparative insights between excavated and stock conditions

Published in European Conference on Fracture (ECF24), Zagreb, Croatia, 2024

A comparative study on hydrogen embrittlement in L485 pipeline materials under excavated and stock conditions, presented at the European Conference on Fracture.

Recommended citation: J. Jubica, L. Claeys, L. De Pue, W. De Waele, T. Depover, and K. Verbeken, "Hydrogen embrittlement in L485 pipeline materials : comparative insights between excavated and stock conditions," in ECF24, European Conference on Fracture, Abstracts, Zagreb, Croatia, 2024.
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The role of hydrogen on the fracture micro-mechanism of different pipeline steels and their welds

Published in EPRI Workshop on Hydrogen Embrittlement 2024, Oxford, the UK, 2024

A study on the role of hydrogen on the fracture micro-mechanism of different pipeline steels and their welds, as presented at the EPRI Workshop on Hydrogen Embrittlement.

Recommended citation: M. Cauwels et al., "The role of hydrogen on the fracture micro-mechanism of different pipeline steels and their welds," in EPRI Workshop on Hydrogen Embrittlement 2024, Abstracts, Oxford, the UK, 2024.
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Screening the hydrogen compatibility of pipeline steels and welds

Published in European Gas Technology Conference 2024 (EGATEC 2024), Hamburg, Germany, 2024

This study aims to develop a fast screening method to evaluate hydrogen embrittlement sensitivity in pipeline steels and their welds for safe hydrogen transport.

Recommended citation: J. Jubica et al., "Screening the hydrogen compatibility of pipeline steels and welds," in European Gas Technology Conference 2024, Book of Abstracts, Hamburg, Germany, 2024.
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Study of the susceptibility of L485 pipeline steel to hydrogen embrittlement

Published in European PhD Hydrogen Conference 2024 (EPHyC 2024), Ghent, Belgium, 2024

This work aims to study fracture patterns and characteristics of L485 pipeline steel samples to understand the underlying causes of material failure due to hydrogen embrittlement.

Recommended citation: J. Jubica et al., "Study of the susceptibility of L485 pipeline steel to hydrogen embrittlement," in European PhD Hydrogen Conference 2024: book of abstracts, Ghent, Belgium, 2024.
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2023

Fractographic study for screening the hydrogen compatibility of X70 pipeline steels and welds

Published in IHC2023 : International Hydrogen Conference, Park City, Utah, USA, 2023

Fractographic study for screening the hydrogen compatibility of X70 pipeline steels and welds, presented at the International Hydrogen Conference 2023.

Recommended citation: L. Claeys et al., "Fractographic study for screening the hydrogen compatibility of X70 pipeline steels and welds," in IHC2023 : International Hydrogen Conference, Abstracts, Park City, Utah, USA, 2023.
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Fractography of Hydrogen-Charged X70 Pipeline Steels under Quasi-Static Tension

Published in EUROCORR 2023, Brussels, Belgium, 2023

This work investigates the fractography of hydrogen-charged X70 pipeline steels under quasi-static tension. It analyzes microstructure, hydrogen content, diffusivity, and fracture modes in base metals and welds. Key features such as dimples, delamination, fisheyes, and quasi-cleavage regions were characterized, providing insights into hydrogen embrittlement mechanisms in pipeline steels.

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Fractographic study of quasi-static tensile tested, electrochemically hydrogen charged X70 pipeline steels

Published in EUROCORR 2023, European Corrosion Congress, Proceedings, Brussels, Belgium, 2023

This work discusses different features identified on quasistatic tensile tested, electrochemically hydrogen charged X70 pipeline steel.

Recommended citation: J. Jubica et al., "Fractographic study of quasi-static tensile tested, electrochemically hydrogen charged X70 pipeline steels," in EUROCORR 2023, European Corrosion Congress, Proceedings, Brussels, Belgium, 2023.
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Microstructural and fractographic investigation of hydrogen embrittlement sensitivity of X70 pipeline steels

Published in 3rd Benelux Network Meeting and Workshop on Damage and Fracture Mechanics (BDFM-2023), Antwerp, Belgium, 2023

Microstructural and fractographic investigation of hydrogen embrittlement sensitivity of X70 pipeline steels, presented at the 3rd Benelux Network Meeting and Workshop on Damage and Fracture Mechanics.

Recommended citation: J. Jubica et al., "Microstructural and fractographic investigation of hydrogen embrittlement sensitivity of X70 pipeline steels," in 3rd Benelux Network Meeting and Workshop on Damage and Fracture Mechanics (BDFM-2023), Abstracts, Antwerp, Belgium, 2023.
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Presentations


2024

Screening Hydrogen Compatibility of Pipeline Steels and Welds

Published in EPRI Workshop on Hydrogen Embrittlement 2024, Jesus College, Oxford, UK, 2024

A poster presentation focusing on a fast, less expensive screening methodology to assess the susceptibility of X70 pipeline steels and their welds to hydrogen embrittlement. This work also investigated the role of gaseous inhibitors in mitigating hydrogen-accelerated crack growth.>

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Books


2020

Characterization of Secondary Carbides in Low-Alloyed Martensitic Model Alloy Tool Steels

Published in Swerim AB, KTH Royal Institute of Technology, 2020

This master thesis studies tool steels with iron, carbon, molybdenum, and vanadium to understand carbide effects on hardness. Two alloys were tempered at 550C and 600C, with hardness measured and compared. Alloy A was analyzed with STEM EDS and TC Prisma simulations, showing molybdenum carbides increase strength. Hardness was higher at 550C due to reduced overaging at 600C.

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